Analytical methods evaluation and validation for vinylidene fluoride, vinyl bromide, vinyl fluoride, benzene.

Details

• Personal Author:
  Dillon HK
• Description:
  Methods for the personal monitoring of vinylidene-fluoride (75387), vinyl-fluoride (75025), vinyl-bromide (593602), benzenethiol (108985), and n-octanethiol were sought. Satisfactory methods for vinyl-bromide and n-octanethiol were developed. The method for the former involved adsorption of the compound on activated coconut charcoal, desorption with ethanol, and determination by gas chromatography with flame ionization detection. The method for the latter involved the collection of the compound on polymer of 2,6- diphenyl-p-phenylene oxide, desorption with acetone, and determination by gas chromatography with sulphur specific flame photometric detection. Methods developed for the other compounds were only partially successful. The author suggests avenues for future development. [Description provided by NIOSH]
• Content Notes:
  in NTRL, no PDF
• Subjects:
  Environmental Monitoring Occupational Health Plastics Safety
• Keywords:
  NIOSH-Contract; Contract-210-79-0100; Plastics; Air-monitoring; Analytical-models; Air-sampling; Sampling-methods; Analytical-processes
• Document Type:
  Text
• Funding:
  Contract
• Genre:
  Report
• Place as Subject:
  Alabama ; Ohio ; OSHA Region 4 ; OSHA Region 5
• CIO:
  National Institute for Occupational Safety and Health (NIOSH)
• Topic:
  Workplace Safety & Health
• Location:
  North America
• Pages in Document:
  1-21
• NIOSHTIC Number:
  nn:00122123
• NTIS Accession Number:
  PB92128693
• Citation:
  NIOSH 1982 Jan; :1-21
• CAS Registry Number:
  Bromoethene (CAS RN 593-60-2) ; Fluoroethylene (CAS RN 75-02-5) ; Thiophenol (CAS RN 108-98-5) ; Vinylidene fluoride (CAS RN 75-38-7)
• Federal Fiscal Year:
  1982
• Peer Reviewed:
  False
• Source Full Name:
  Southern Research Institute, Birmingham, Alabama, NIOSH, Cincinnati, Ohio, 21 pages, 3 references
• Collection(s):
  National Institute for Occupational Safety and Health
• Main Document Checksum:
  urn:sha-512:7dc847c09aedf140bc731323e8446b4703641ae07d6ad9e7b7238120dab30b8f7dcaa9b938d34d035f87873a0fe7fec262d5d13dcaf290925445e82b6de3b57d
• Download URL:
  https://stacks.cdc.gov/view/cdc/241420/cdc_241420_DS1.pdf
• File Type:
  [PDF - 168.02 KB ]