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NIOSH Manual of Analytical Methods [NMAM] 4th Edition [database]
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1994/08/01
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Alternative Title:NIOSH Manual of Analytical Methods [NMAM]: 4th Edition
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Description:NMAM is a collection of methods for sampling and analysis of contaminants in workplace air, and in the blood and urine of workers who are occupationally exposed. These methods have been developed or adapted by NIOSH or its partners and have been evaluated according to established experimental protocols and performance criteria. NMAM also includes chapters on quality assurance, sampling, portable instrumentation, etc. NIOSH recommends that the best method available be used for making each measurement. Methods published by others, such as OSHA, MSHA, EPA, ASTM, ISO or commercial suppliers of sampling and analytical equipment, may have advantages over NIOSH methods for a given sampling situation. (An Industrial Hygienist should determine the sampling protocol, considering analytical accuracy, cost, and optimum sample number.) Every method should undergo an initial evaluation to demonstrate performance. When a method is used in a laboratory that did not perform the initial evaluation, that laboratory should verify that comparable results can be obtained. NIOSH methods may need to be modified, and if modified, should be re-evaluated. Various OSHA regulations (e.g. benzene) mention performance criteria for evaluating whatever method is used. NIOSH has published methods developed in cooperating laboratories. These method performance have been evaluated using established experimental protocols. These methods were selected based upon priorities established in a joint NIOSH/AIHA survey of participating laboratories.
Methods in the 4th Edition include: 250: Nitroglycerin; 500: Particulates Not Otherwise Regulated, Total ; 600: Particulates Not Otherwise Regulated, Respirable; 1000: Allyl Chloride; 1001: Methyl Chloride; 1002: B-Chloroprene; 1003: Hydrocarbons, Halogenated; 1004: Dichloroethyl Ether; 1005: Methylene Chloride; 1006: Fluorotrichloromethane; 1007: Vinyl Chloride; 1008: Ethylene Dibromide; 1009: Vinyl Bromide; 1010: Epichlorohydrin; 1011: Ethyl Bromide; 1012: Difluorodibromomethane; 1013: Propylene Dichloride; 1014: Methyl Iodide; 1015: Vinylidene Chloride; 1016: (1) 1,1, 1,2-Tetrachloro-2,2-Difluoroethane and 1016 (2) 1,1, 2,2-Tetrachloro-1,2-Difluoroethane; 1017: Trifluorobromomethane; 1018: Dichlorodifluoromethane; 1019: 1,1, 2,2-Tetrachloroethane; 1020: 1,1, 2-Trichloro-1,2, 2-Trifluoroethane; 1022: Trichloroethylene; 1024: 1,3-Butadiene; 1025: 1- and 2-Bromopropane; 1026: P-Chlorobenzotrifluoride; 1300: Ketones I; 1301: Ketones II; 1302: N-Methyl-2-Pyrrolidinone; 1400: Alcohols I; 1401: Alcohols II; 1402: Alcohols III; 1403: Alcohols IV; 1404: Methylcyclohexanol; 1405: Alcohols Combined; 1450: Esters; 1451: Methyl Cellosolve Acetate; 1452: Ethyl Formate; 1454: Isopropyl Acetate; 1457: Ethyl Acetate; 1458: Methyl Acetate; 1459: Methyl Acrylate; 1460: Isopropyl Acetate; 1500: Hydrocarbons, BP 36ø-216 øC; 1501: Hydrocarbons, Aromatic; 1550: Naphthas; 1551: Turpentine; 1552: Terpenes; 1600: Carbon Disulfide; 1601: 1,1-Dichloro-1-Nitroethane; 1602: Dioxane; 1603: Acetic Acid; 1604: Acrylonitrile; 1606: Acetonitrile; 1608: Glycidol; 1609: Tetrahydrofuran; 1610: Ethyl Ether; 1611: Methylal; 1612: Propylene Oxide; 1613: Pyridine; 1614: Ethylene Oxide; 1615: Methyl Tert-Butyl Ether; 1616: N-Butyl Glycidyl Ether; 1617: Phenyl Ether; 1618: Isopropyl Ether; 1619: Phenyl Glycidyl Ether; 1620: Isopropyl Glycidyl Ether; 2000: Methanol; 2002: Amines, Aromatic; 2003: 1,1, 2,2-Tetrabromoethane; 2004: Dimethylacetamide; 2005: Nitroaromatic Compounds; 2007: Aminoethanol Compounds I; 2008: Chloroacetic Acid; 2010: Amines, Aliphatic; 2011: Formic Acid; 2012: N-Butylamine; 2013: Phenyl Ether-Diphenyl Mixture; 2014: P-Chlorophenol; 2015: Chloroacetaldehyde; 2016: Formaldehyde; 2017: Aniline, O-Toluidine, and Nitrobenzene; 2018: Aliphatic Aldehydes; 2500: Methyl Ethyl Ketone; 2501: Acrolein; 2503: Mevinphos; 2504: Tetraethyl Pyrophosphate; 2505: Furfuryl Alcohol; 2506: Acetone Cyanohydrin; 2507: Ethylene Glycol Dinitrate; 2508: Isophorone; 2510: 1-Octanethiol; 2513: Ethylene Chlorohydrin; 2514: Anisidine; 2515: Diazomethane; 2516: Dichlorofluoromethane; 2517: Pentachloroethane; 2518: Hexachloro-1,3-Cyclopentadiene; 2519: Ethyl Chloride; 2520: Methyl Bromide; 2521: Methylcyclohexanone; 2522: Nitrosamines; 2523: 1,3-Cyclopentadiene; 2524: Dimethyl Sulfate; 2525: N-Butyl Mercaptan; 2526: Nitroethane; 2527: Nitromethane; 2528: 2-Nitropropane; 2529: Furfural; 2530: Diphenyl; 2531: Glutaraldehyde; 2532: Glutaraldehyde; 2533: Tetraethyl Lead (as Pb); 2534: Tetramethyl Lead (as Pb); 2535: Toluene-2,4-Diisocyanate; 2536: Valeraldehyde; 2537: Methyl and Ethyl Methacrylate; 2538-1: Acetaldehyde by GC; 2538: Acetaldehyde; 2539: Aldehydes, Screening; 2540: Ethylenediamine; 2540-1: Triethylenetetramine; 2540-2: Ethylenediamine; 2540-deta: Diethylenetriamine; 2540-teta: Triethylenetetramine; 2541: Formaldehyde by GC; 2542: Mercaptans, Methyl-, Ethyl-, and N-Butyl; 2543: Hexachlorobutadiene; 2544: Nicotine; 2545: Allyl Glycidyl Ether; 2546: Cresol (All Isomers) and Phenol; 2549: Volatile Organic Compounds (Screening); 2550: Benzothiazole in Asphalt Fume; 2551: Nicotine; 2552: Methyl Acrylate; 2553: Ketones II; 2554: Glycol Ethers; 2555: Ketones I; 2556: Isophorone; 2557: Diacetyl; 2558: Acetoin; 2559: Decabromodiphenyl Oxide; 2560: 1-Nitropyrene in Diesel Particulates; 2561: (1) 2-(Dimethylamino)ethanol, (2) 1-Dimethylamino-2-Propanol; 2562: 1,1, 2,2-Tetrachloroethane; 3500: Formaldehyde by VIS; 3502: Phenol; 3503: Hydrazine; 3505: Tetramethyl Thiourea; 3506: Acetic Anhydride; 3507: Acetaldehyde by HPLC; 3507-1: Acetaldehyde; 3508: Methyl Ethyl Ketone Peroxide; 3509: Aminoethanol Compounds II; 3510: Monomethylhydrazine; 3511: Monomethylaniline; 3512: Maleic Anhydride; 3513: Tetranitromethane; 3514: Ethylenimine; 3515: 1,1-Dimethylhydrazine; 3516: Crotonaldehyde; 3518: Phenylhydrazine; 3600: Maneb; 3601: Maneb Hand Wash; 3700: Benzene by Portable GC; 3701: Trichloroethylene by Portable GC; 3702: Ethylene Oxide by Portable GC; 3704: Perchloroethylene (Portable GC); 3800: Organic and Inorganic Gases by Extractive FTIR Spectrometry; 4000: Toluene (Diffusive Sampler); 5000: Carbon Black; 5001-24-D: 2,4-D; 5001-245T: 2,4, 5-T; 5002: Warfarin; 5003: Paraquat; 5004: Hydroquinone; 5005: Thiram; 5006: Carbaryl; 5007: Rotenone; 5008: Pyrethrum; 5009: Benzoyl Peroxide; 5010: (1) Bromoxynil and (2) Bromoxynil Octanoate; 5011: Ethylene Thiourea; 5012: EPN; 5013: Dyes, Benzidine-, O-Tolidine-, O-Dianisidine; 5014: Chlorinated Terphenyl (60% Chlorine); 5016: Strychnine; 5017: Dibutyl Phosphate; 5018: 2,4, 7-Trinitrofluoren-9-One; 5019: Azelaic Acid; 5020: DI(2-Ethylhexyl) Phthalate, See Dibutyl Phthalate (Method); 5020HEX: DI(2-Ethylhexyl) Phthalate; 5021: O-Terphenyl; 5022: Arsenic, Organo; 5023: Coal Tar Pitch Volatiles; 5025: Chlorinated Diphenyl Oxide; 5026: Oil Mist, Mineral; 5027: Ribavirin; 5029: 4,4′-Methylenedianiline; 5030: Cyanuric Acid; 5031: Aspartame; 5032: Pentamidine Isethionate; 5033: P-Nitroaniline; 5034: Tributyl Phosphate; 5035: Super Absorbent Polymers; 5036: Trimellitic Anhydride; 5037: Triorthocresyl Phosphate; 5038: Triphenyl Phosphate; 5039: Chlorinated Camphene; 5041: Capsaicin and Dihydrocapsaicin; 5042: Benzene-Soluble Fraction and Total Particulate (Asphalt Fumes); 5043: P-Toluenesulfonic Acid; 5044: Estrogenic Compounds; 5046: Tetrakis(hydroxymethyl)phosphonium Chloride; 5500: Ethylene Glycol; 5502ALD: Aldrin; 5502LIN: Lindane; 5503: Polychlorobiphenyls; 5504: Organotin Compounds (as Sn); 5506: Polynuclear Aromatic Hydrocarbons by HPLC; 5508: Kepone; 5509: Benzidine; 5510: Chlordane; 5512: Pentachlorophenol; 5514: Demeton; 5515: Polynuclear Aromatic Hydrocarbons by GC; 5516: 2,4- and 2,6-TOLUENEDIAMINE(in the Presence of Isocyanates); 5517: Polychlorobenzenes; 5518: Naphthylamines, A and B; 5519: Endrin; 5521: Isocyanates, Monomeric; 5522: Isocyanates; 5523: Glycols; 5525: Isocyanates, Total (Map); 5526: Methyltin Chlorides; 5527: Triphenyl Tin Chloride (as Sn); 5600: Organophosphorus Pesticides; 5601: Organonitrogen Pesticides; 5602: Chlorinated and Organonitrogen Herbicides (Air Sampling); 5603: Alachlor in Air; 5606: Thiophanate-Methyl in Air; 5700: Formaldehyde on Dust (Textile or Wood); 5701: Resorcinol; 5733: Coal Tar Pitch Volatiles; 6001: Arsine; 6002: Phosphine; 6004: Sulfur Dioxide; 6005: Iodine; 6006: Diborane; 6007: Nickel Carbonyl; 6008: Stibine; 6009: Mercury; 6010: Hydrogen Cyanide; 6011: Bromine 6011 Now Available in NMAM 5th Edition; 6012: Sulfuryl Fluoride; 6013: Hydrogen Sulfide; 6014: Nitric Oxide and Nitrogen Dioxide; 6015: Ammonia; 6016: Ammonia by IC; 6017: Hydrogen Cyanide; 6402: Phosphorus Trichloride; 6600: Nitrous Oxide; 6601: Oxygen; 6602: Sulfur Hexafluoride by Portable GC; 6603: Carbon Dioxide; 6604: Carbon Monoxide; 6700: Nitrogen Dioxide (Diffusive Sampler); 7013: Aluminum and Compounds, as Al; 7020: Calcium and Compounds, as Ca; 7024: Chromium and Compounds, as Cr; 7027: Cobalt and Compounds, as Co; 7029: Copper (Dust and Fumes); 7030: Zinc and Compounds, as Zn; 7048: Cadmium and Compounds, as CD; 7056: Barium, Soluble Compounds; 7074: Tungsten (Soluble and Insoluble); 7082: Lead by Flame AAS; 7102: Beryllium and Compounds, as Be; 7105: Lead by GFAAS; 7300: Elements by ICP (Nitric/Perchloric Acid Ashing); 7301: Elements by ICP; 7303: Elements by ICP (Hot Block/HCl/HNO3 Digestion); 7400: Asbestos and Other Fibers by PCM 7400 Now Available in NMAM 5th Edition; 7401: Alkaline Dusts, NaOH, Koh, LiOH, and Basic Salts; 7402: Asbestos by TEM 7402 Now Available in NMAM 5th Edition; 7404: Cellulose Insulation; 7500: Silica, Crystalline, by XRD (Filter Redeposition); 7501: Silica, Amorphous; 7502: Zinc Oxide; 7504: Vanadium Oxides; 7505: Lead Sulfide; 7506: Boron Carbide; 7600: Chromium, Hexavalent; 7601: Silica, Crystalline, by VIS; 7602: Silica, Crystalline by IR (KBr Pellet); 7603: Quartz in Coal Mine Dust, by IR (Redeposition); 7605: Chromium, Hexavalent; 7701: Lead by Portable Ultrasonic Extraction/ASV; 7702: Lead by Field Portable XRF; 7703: Chromium, Hexavalent, by Field-Portable Spectrophotometry; 7900: Arsenic and Compounds, as AS (Except AsH3 and As2O); 7901: Arsenic Trioxide, as AS; 7902: Fluorides, Aerosol and Gas by Ise; 7903: Acids, Inorganic; 7904: Cyanides, Aerosol and Gas; 7905: Phosphorus; 8001: Pentachlorophenol in Blood; 8002: Methyl Ethyl Ketone, Ethanol, and Toluene in Blood; 8003: Lead in Blood and Urine; 8004: Polychlorobiphenyls in Serum; 8005: Elements in Blood or Tissue; 8300: Hippuric Acid in Urine; 8301: Hippuric and Methyl Hippuric Acids in Urine; 8302: MBOCA in Urine; 8303: Pentachlorophenol in Urine; 8304: Benzidine in Urine (Screening Test; 8305: Phenol and P-Cresol in Urine; 8306: Benzidine in Urine; 8308: Fluoride in Urine; 8310: Metals in Urine; 8315: Triazine Herbicides and Their Metabolites in Urine; 8316: Butoxyacetic Acid in Urine; 8317: Aniline and @-Toluidine in Urine; 9000: Asbestos, Chrysotile by XRD; 9002: Asbestos (Bulk) by PLM; 9100: Lead in Surface Wipe Samples; 9101: Chromium, Hexavalent, in Settled Dust Samples; 9102: Elements on Wipes; 9105: Lead in Dust Wipes by Chemical Spot Test (Colorimetric Screening Method); 9200: Chlorinated and Organonitrogen Herbicides (Hand Wash); 9201: Chlorinated and Organonitrogen Herbicides (Patch); 9202: Captan and Thiophanate-Methyl in Handrinse; and, 9205: Captan and Thiophanate-Methyl on Dermal Patch.
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Content Notes:This record describes only the online 4th Edition database encompassing all editions. The original print edition and the three (3) Supplements are linked to this record. Find the links in the "Related" items below.
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Contributor:Doemeny, Laurence J.;Fannin, Grace A.;Elfers, Deanna L.;
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NIOSHTIC Number:20000064
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Citation:Cincinnati, OH: U.S. Department of Health and Human Services, Public Health Service, Centers for Disease Control and Prevention, National Institute for Occupational Safety and Health, DHHS (NIOSH) Publication No. 94-113, 1994 August; : Database
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Federal Fiscal Year:1994
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Peer Reviewed:False
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Resource Number:DHHS (NIOSH) Publication No. 94-113;DHHS (NIOSH) Publication No. 96-135;DHHS (NIOSH) Publication No. 98-119;DHHS (NIOSH) Publication No. 2003-154;
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