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NIOSH Manual of Analytical Methods (NMAM), 5th Edition [print edition]
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2020/02/01
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Alternative Title:NIOSH Manual of Analytical Methods (NMAM), 5th Edition
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Description:The National Institute for Occupational Safety and Health (NIOSH) is the U.S. federal agency responsible for conducting research and making recommendations for the prevention of work-related injury and illness. NIOSH is part of the Centers for Disease Control and Prevention (CDC) in the U.S. Department of Health and Human Services. The NIOSH Manual of Analytical Methods (NMAM) is a compilation of validated sampling and analytical methods that are used globally for occupational exposure assessment in the industrial (occupational) hygiene field and related professions. The methods that are published in NMAM are evaluated and validated in consideration of their fitness-for-purpose for exposure monitoring in work areas. NIOSH methods primarily address workplace air sampling and analysis, but NMAM also includes protocols for biological, surface, dermal, and bulk samples. Within NMAM, but separate from the methods themselves, are assorted chapters providing background and guidance covering a number of subjects. Explanatory chapters on quality assurance, sampling guidance, method development and evaluation, aerosol collection, etc., provide valuable information to users of NIOSH methods. NMAM chapters provide a convenient resource that augments technical information often (but not always) available elsewhere in texts and monographs. Now in its fifth edition, NMAM is continuously updated as new or revised methods are evaluated and their performance verified. This document is a compilation of its guidance chapters and methods, current as of the date shown on the front page. NMAM is published online at https://www.cdc.gov/niosh/nmam/ and is available worldwide free of charge. Users are encouraged to visit the NMAM 5th edition website for the most current methods and guidance chapters.
The 72 Methods included are: 501: Particulates N.O.R., Total
1453: Vinyl Acetate
2005: Nitroaromatic Compounds
2008: Chloroacetic Acid
2014: P-Chlorophenol
2016: Formaldehyde
2027: Ketones
2514: Anisidine
2520: Methyl Bromide
2531: Glutaraldehyde
2536: Valeraldehyde
3800: Organic & Inorganic Gases by Extractive FTIR Spectrometry
3900: Volatile Organic Compounds, C1 to C10, Canister Method
5004: Hydroquinone
5005: Thiram
5007: Rotenone
5008: Pyrethrum
5009: Benzoyl Peroxide
5016: Strychnine
5022: Arsenic, Organo-
5033: P-Nitroaniline
5040: Diesel Particulate Matter (as Elemental Carbon)
5100: Carbon Black
5504: Organotin Compounds (as Sn)
5509: Benzidine and 3,3′-Dichlorobenzidine
5524: Metalworking Fluids (MWF) All Categories
5526: Methyltin Chlorides
5528: Polynuclear Aromatic Hydrocarbons in Air by GC-MS Sim
5600: Organophosphorus Pesticides
5601: Organonitrogen Pesticides
5700: Formaldehyde on Dust (Textile or Wood)
6001: Arsine
6002: Phosphine
6010: Hydrogen Cyanide
6012: Sulfuryl Fluoride
6016: Ammonia by IC
6604: Carbon Monoxide
7082: Lead by Flame AAS
7302: Elements by ICP (Microwave Digestion)
7304: Elements by ICP Microwave Digestion
7306: Elements by Cellulosic Internal Capsule Sampler
7400: Asbestos and Other Fibers by PCM
7402: Asbestos by TEM
7405: Alkali Metal Cations Na+, K+, Li+
7502: Zinc Oxide
7600: Chromium, Hexavalent
7602: Silica, Respirable Crystalline, by IR (KBr Pellet)
7603: Quartz in Respirable Coal Mine Dust, by IR (Redeposition)
7605: Chromium, Hexavalent by Ion Chromatography
7701: Lead by Portable Ultrasonic Extraction/ASV
7703: Chromium, Hexavalent by Field-Portable Spectrophotometry
7704: Beryllium in Air by Fluorometry
7906: Particulate Fluorides and Hydrofluoric Acid by Ion Chromatography
7907: Volatile Acids by Ion Chromatography
7908: Non-Volatile Acids (Sulfuric Acid and Phosphoric Acid – Previous Issue)
8007: Toluene in Blood
8200: Elements in Tissues
8308: Fluoride in Urine
8318: 2,5-Hexanedione in Urine
8319: Acetone and Methyl Ethyl Ketone in Urine
8320: Butyltin Trichloride in Urine
8321: O-Cresol in Urine
8322: Trichloroacetic Acid in Urine
8324: 3-Bromopropionic Acid in Urine
8326: S-Benzylmercapturic Acid and S-Phenylmercapturic Acid in Urine
8327: Cyclophosphamide, 4-Ketocyclophosphamide and Ifosfamide in Urine
9000: Asbestos, Chrysotile by XRD
9106: Methamphetamine and Illicit Drugs, Precursors and Adulterants on Wipes by Liquid-Liquid Extraction
9109: Methamphetamine and Illicit Drugs, Precursors and Adulterants on Wipes by Solid-Phase Extraction
9110: Beryllium in Surface Wipes by Fluorometry
9111: Methamphetamine on Wipes by LC/MS
and, 9212: Mitomycin C.
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Content Notes:Stacks staff added the 4 Methods missing from the NIOSH webbook on 2025-02-12. The 3 earlier versions of the 5th Edition Webbook are included in the Supporting Files section for reference and complete representation.
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Pages in Document:980 pdf pages
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Contributor:Barton, Giles;Barton, Nancy;Collins, Seleen;Schwegler-Berry, Diane;Shoemaker, D.A.;Turkevich, Leonid;
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NIOSHTIC Number:nn:20069901
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Citation:Andrews R, O'Connor PF, eds. Cincinnati, OH: U.S. Department of Health and Human Services, Public Health Service, Centers for Disease Control and Prevention, National Institute for Occupational Safety and Health, 2020 Feb;:1-935;
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Federal Fiscal Year:2020
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Peer Reviewed:False
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