Failure report no. S373.

Details

• Corporate Authors:
  National Institute for Occupational Safety and Health
• Description:
  Attempts to devise a method (S373) for analyzing methyl-mercaptan (74931) are described. The proposed method involved collection in a solid sorbent tube, desorption with solvent, and analysis by gas chromatography with a flame photometric detector in the sulfur (7704349) operation mode. Other methods tested for n-butyl- mercaptan and ethyl-mercaptan were reviewed. Development of the proposed method was discontinued, since results of other mercaptan analysis reports indicated poor recovery and stability rates, and lack of specificity. [Description provided by NIOSH]
• Content Notes:
  in NTRL, no PDF
• Subjects:
  Chemistry Occupational Health Safety Solvents Sulfur Compounds
• Keywords:
  Chemical-properties; Gas-chromatography; Flame-photometry; Solvents; Organo-sulfur-compounds
• Document Type:
  Text
• Genre:
  Report
• Place as Subject:
  Ohio ; OSHA Region 5
• CIO:
  National Institute for Occupational Safety and Health (NIOSH)
• Topic:
  Workplace Safety & Health
• Location:
  North America
• Pages in Document:
  1-3
• NIOSHTIC Number:
  nn:00107262
• NTIS Accession Number:
  PB81240715
• Citation:
  NIOSH; :1-3
• CAS Registry Number:
  Methanethiol (CAS RN 74-93-1) ; Sulfur (CAS RN 7704-34-9)
• Peer Reviewed:
  False
• Source Full Name:
  NIOSH, Unpublished, Cincinnati, Ohio, 3 pages, 4 references
• Collection(s):
  National Institute for Occupational Safety and Health
• Main Document Checksum:
  urn:sha-512:7dc847c09aedf140bc731323e8446b4703641ae07d6ad9e7b7238120dab30b8f7dcaa9b938d34d035f87873a0fe7fec262d5d13dcaf290925445e82b6de3b57d
• Download URL:
  https://stacks.cdc.gov/view/cdc/241205/cdc_241205_DS1.pdf
• File Type:
  [PDF - 168.02 KB ]