Analytical services for special measurement problems.

Details

• Personal Author:
  Holtz J
• Description:
  Efforts in the area of analytical services to NIOSH for special measurement problems are summarized. Samples were difficult to analyze and outside the scope of typical analytical problems handled by NIOSH laboratories. Twenty-three benzene (71432) soluble extracts for filters containing coal-tar pitch volatiles were submitted. Each extract was quantitatively analyzed for acridine (260946), benzol(a)pyrene (50328), and beta-naphthylamine (91598). Eight lacquer thinner samples were analyzed qualitatively for isopropyl-alcohol (67630), isopropyl-acetate (108214), methylethylketone (78933), methylisobutylketone (108101), isobutyl- alcohol (78831), isobutylacetate (110190), propylacetate (109604), butylacetate (123864), toluene (108883), xylenes/M, O, P-isomers (1330207), benzene, and 3-methylhexone. Three pentachorophenol samples were analyzed for 2,3,7,8-tetrachlorodibenzo-p-dioxin (TCDD) using gas-chromatography via electron capture. A detergent sample was analyzed for monoethanolaminedodecyl-benzene-sulfonate , o- benzyl-p-chlorophenol, tetrasodium-ethylenediaminetetra-acetate , isopropanol, benzene, toluene, and water. The analytical procedures for each element are listed. [Description provided by NIOSH]
• Content Notes:
  in NTRL, no PDF
• Subjects:
  Acetates Amines Chemistry Chemistry, Analytic Hydrocarbons Occupational Health Phenol Polycyclic Aromatic Hydrocarbons Safety Solvents
• Keywords:
  NIOSH-Contract; Contract-099-74-0102; Analysis; Analytical-methods; Analytical-chemistry; Activation-analysis; Neutron-activation-analysis; Solvents; Organic-solvents; Aromatic-hydrocarbons; Hydrocarbons; Amines; Acetates; Alcohols; Phenols
• Document Type:
  Text
• Funding:
  Contract
• Genre:
  Report
• Place as Subject:
  Ohio ; OSHA Region 5
• CIO:
  National Institute for Occupational Safety and Health (NIOSH)
• Topic:
  Workplace Safety & Health
• Location:
  North America
• Pages in Document:
  1-8
• NIOSHTIC Number:
  nn:00080662
• NTIS Accession Number:
  PB82142712
• Citation:
  NIOSH 1975 Nov; :1-8
• CAS Registry Number:
  2-Naphthylamine (CAS RN 91-59-8) ; Acridine (CAS RN 260-94-6) ; Benzene (CAS RN 71-43-2) ; Benzo[a]pyrene (CAS RN 50-32-8) ; Butyl acetate (CAS RN 123-86-4) ; Isobutanol (CAS RN 78-83-1) ; Isobutyl acetate (CAS RN 110-19-0) ; Isopropanol (CAS RN 67-63-0) ; Isopropyl acetate (CAS RN 108-21-4) ; Methyl ethyl ketone (CAS RN 78-93-3) ; Methyl isobutyl ketone (CAS RN 108-10-1) ; Propyl acetate (CAS RN 109-60-4) ; Toluene (CAS RN 108-88-3) ; Xylene (CAS RN 1330-20-7)
• Federal Fiscal Year:
  1976
• Peer Reviewed:
  False
• Source Full Name:
  NIOSH, Cincinnati, Ohio, Final Report
• Collection(s):
  National Institute for Occupational Safety and Health
• Main Document Checksum:
  urn:sha-512:7dc847c09aedf140bc731323e8446b4703641ae07d6ad9e7b7238120dab30b8f7dcaa9b938d34d035f87873a0fe7fec262d5d13dcaf290925445e82b6de3b57d
• Download URL:
  https://stacks.cdc.gov/view/cdc/240785/cdc_240785_DS1.pdf
• File Type:
  [PDF - 168.02 KB ]